Ultrafast high-resolution magic-angle-spinning NMR spectroscopy.
نویسندگان
چکیده
We demonstrate the acquisition of ultrafast 2D NMR spectra of semi-solid samples, with a high-resolution magic-angle-spinning setup. Using a recent double-quantum NMR pulse sequence in optimised synchronisation conditions, high-quality 2D spectra can be recorded for a sample under magic-angle spinning. An illustration is given with a semi-solid sample of banana pulp.
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ورودعنوان ژورنال:
- The Analyst
دوره 140 12 شماره
صفحات -
تاریخ انتشار 2015